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EBSD Electron Backscatter Diffraction

EBSD is a technique that uses backscattered electron diffraction to identify the crystallographic orientations of samples. In the semiconductor industry, this technique is often used to study the microstructure of materials. The EBSD probe device is located in a focused ion beam (FIB) microscope, where the sample surface is tilted at an angle of about 70 degrees to the direction of the electron beam. When the electron beam strikes the sample, it generates backscattered electrons that produce diffraction patterns as they pass through the surface crystal structure, forming Kikuchi lines and Kikuchi patterns. This information, which carries the orientation of the surface grains of the sample, enters the detector to determine the orientation of each individual grain.

 

After knowing the diffraction state at each position on the sample surface and the orientation of each grain, this information can be used to further analyze grain boundaries, grain orientations, textures, and strains. It can also be combined with EDX for collaborative analysis, conducting phase identification and distribution analysis.

 

MA-tek hasAdvanced FIB-SEM and EBSD system integration platformcan accurately measure nanometer-level grain structures and combineEDX, TEM, SIMSand multiple analysis techniques to provide customers with comprehensive microstructural analysis and failure root cause determination, assisting in improving product reliability and process yield.

Applications and Examples of EBSD

By analyzing the diffraction signals from various points on the surface of the sample, EBSD can further analyze the following structural features:

    • Grain Boundary AnalysisDetermine the type and angle difference of grain boundaries.

    • Grain OrientationDraw the grain orientation distribution map to reveal the crystal arrangement direction.

    • Texture analysisUnderstand the crystal arrangement tendency of materials during the forming process.

    • Strain distributionDetecting the internal stress concentration and deformation state of materials.

    • Phase Identification & Distributionto matchEDX energy dispersive spectroscopy analysiscan identify the chemical composition and distribution of different phases.

 

EBSD application fields

EBSD technology is widely applied insemiconductors, electronic materials, metals, ceramics, and advanced packagingIn the industry, especially inGrain structure observation, reliability failure analysis, and process optimizationPlay a key role.

EBSD applications include:

  • Substructure Analysis

  • Grain Size / Boundary Characterization

  • Grain Orientation & Texture Analysis

  • Phase Identification & Distribution Mapping

  • Analysis of Material Deformation and Recrystallization Behavior (Deformation & Recrystallization Study)

  • Strain & Stress Distribution

 

EBSD application examples

  • Orientation Map

  • Phase Map

  • Grain size distribution

  • Misotientation angle distribution

  • Pole figure

  • Inverse pole figure

Frequently Asked Questions
What is the acceptable size for samples in EBSD analysis?
A. The general dimensions should not exceed 1cm x 1cm x 0.5cm, but it is recommended to discuss with the technical unit before analysis.
Q2. What are the sample preparation requirements for EBSD?
A. Overall, the analysis surface of the sample must be prepared to be sufficiently flat in order to perform EBSD analysis, as the flatness of the sample will directly affect the quality of EBSD imaging. Different samples have different preparation methods, with common methods including grinding and polishing, electro-polishing, and ion polishing.
Q3. What level of accuracy can the orientation angle between grains reach?
A. Under optimal conditions, it can reach 0.05°.
Q4. What types of samples usually require EBSD analysis?
A. General EBSD is used to analyze materials with crystalline structures. Although TEM and SEM can observe grain morphology and size, they cannot quantify the distribution of grain sizes and the orientation of grain directions; EBSD, on the other hand, has a large scanning range that can cover many grains. In addition to observing grain morphology, it also has the functions of statistically analyzing grain size, grain orientation, phase identification, and their distributions.
Q5. What is the minimum grain size limit that can be analyzed?
A. The current physical limit for EBSD detection of grain size is about 50nm, but the grain size that EBSD can analyze is greatly related to the sample itself and the condition of the sample surface (sample preparation condition); generally speaking, the better the sample surface condition, the more favorable it is for sample analysis.
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